Faith A. Fitzpatrick James D. Blount Leah E.K. Lenoch Sarah A. Francart Allen C. Gellis Barbara C. Eikenberry Heidi M. Broerman Shannon M. Pace 20250821 tabular digital data https://doi.org/10.5066/P13W43BB Faith A. Fitzpatrick James D. Blount Leah E. K. Lenoch Sarah A. Francart Allen C. Gellis Barbara C. Eikenberry 2019 publication Proc. SEDHYD, 2019 (4) (2019), pp. 189-204 https://pubs.usgs.gov/publication/70217015 These datasets include physical and geochemical lab results of sediment samples collected from August 2016 to October 2018. Upland samples were collected at randomly selected sites in the watershed using the geographic information system (GIS) site-selection procedure. Passive suspended-sediment samplers were installed at three sites and sampled monthly. Streambank and streambed sediment were collected, if present at rapid geomorphic assessment (RGA) sites, at eroding banks and areas of soft, fine-grained bed sediment, respectively. Samples underwent a particle size analysis and were analyzed for a suite of trace elements. These results were used in the Sediment Source Assessment Tool (Sed_SAT) to help identify upland and stream corridor sources of suspended and stream bed sediment. These samples were collected and used to identify and apportion source contributions of upland and streambank sources. This information will enable resource managers to improve how different land uses are managed in order to decrease delivery of sediment and the nutrients that travel with this sediment to streams. Ultimately, a decrease in sediment and nutrient concentrations in the East River will decrease what is delivered to the Lower Fox River and Green Bay, preventing the conditions that foster harmful algal blooms. 201608 201810 ground condition Complete None planned -88.2532 -88.0884 44.3361 44.1773 ISO 19115 Topic Category geoscientificInformation None geomorphology geochemistry sediment fingerprinting sediment transport particle size USGS Metadata Identifier USGS:671818b3d34ee1f0a882260c Geographic Names Information Systems (GNIS) Wisconsin Green Bay Wrightstown Brown County United States North America Great Lakes Lake Michigan None. Please see 'Distribution Info' for details. None. Users are advised to read the dataset's metadata thoroughly to understand appropriate use and data limitations. USGS Upper Midwest Water Science Center Center Director mailing and physical

1992 Folwell Ave.

St. Paul MN 55108 United States 608-828-9901 gs-w-umidwsc_center_director@usgs.gov Funding for this study was provided by the Great Lakes Restoration Initiative, U.S. Environmental Protection Agency This dataset was produced on a computer running Windows 10, using the software package Microsoft Excel for Microsoft 365 MSO (Version 2308 Build 16.0.16731.20542) 32-bit. Filenames: Plum_ParticleSize_PhysicalData.csv 15 KB Plum_SedSAT_GeochemicalData.csv 92 KB Particle size and organic matter determinations were completed at the USGS Cascades Laboratory in Vancouver, Washington. Elemental analyses were conducted at the Wisconsin State Laboratory of Hygiene in Madison, Wisconsin. A known replicate sample was run with each batch with each lab for quality assurance (QA). No formal logical accuracy tests were conducted. Data are considered complete for the information presented, as described in the abstract. Specific sample locations are not included to protect the anonymity of landowners who allowed samples to be collected on their property as part of this study; contact the Upper Midwest Water Science Center center director for more information. Users are advised to read the rest of the metadata carefully for additional details. No formal positional accuracy tests were conducted. No formal positional accuracy tests were conducted. The Plum_SedSAT_GeochemicalData dataset contains the lab analysis results for elemental data in field collected upland, suspended sediment, streambank, and streambed samples in the study area. Wisconsin State Laboratory of Hygiene used the ESS INO Method 420.0 Thermo Finnigan ELEMENT2 High Resolution ICP-MS (EPA Method 200.8) method and the milestone microwave digestion system (ESS INO IOP 550.0) for elemental analyses (Wisconsin State Laboratory of Hygiene 2016a; 2016b). The elemental analysis included a near total digestion using three acids. Data is also available at the Wisconsin Department of Natural Resources Surface Water Integrated Monitoring System (SWIMS) Database; Wisconsin DNR users and external users with a Web Access Management System (WAMS) account can access the database at https://apps.dnr.wi.gov/swims/Projects/ProjectDetail?id=129143166. This dataset is formatted for use with the Sediment Source Apportionemtn Tool (Sed_SAT). 2024 Faith A Fitzpatrick U.S. Geological Survey, MIDCONTINENT REGION Research Hydrologist mailing

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Madison WI 53726 US 608-821-3818 fafitzpa@usgs.gov The Plum_ParticleSize_PhysicalData dataset contains the lab analysis results for particle size data in field collected upland, suspended sediment, streambank, and streambed samples in the study area. Samples were wet sieved with a 63 micrometer Teflon sieve so that tests were conducted on the less than 63 micrometer fraction of the sample. USGS Cascades Laboratory analyzed the samples using a SediGraph 5120 for particle size distribution, and I-5753 method for loss on ignition (LOI) to analyze organic matter content. The attributes D50_calulated and LOI_mg_kg are recorded in the Plum_SedSAT_GeochemicalData dataset as it was formatted for use in the Sediment Source Apportionemnt Tool (Sed_SAT). 2024 Faith A Fitzpatrick U.S. Geological Survey, MIDCONTINENT REGION Research Hydrologist mailing

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Madison WI 53726 US 608-821-3818 fafitzpa@usgs.gov Plum_ParticleSize_PhysicalData.csv D84, D50, particle size distribution, and LOI data. All particle sizes are measured in millimeters unless defined otherwise in the attribute definition. Producer Defined FullName The sample name, completely written out. Producer Defined Recorded by basin, sample type, and sample number [Plum - Type - ##] format. Samples without sample numbers are either in [Plum - Type] or [Plum - Type - Location in Basin] format. These samples are differentiated by their collection date. Sample_ID Identification code of the sample analyzed. Producer Defined Identification code, recorded in basin, sample type, sample number, and collection date [PLCType##YYYYMMDD] format. Samples with out a sample number are in [PLCTypeYYYYMMDD] format. Date_YYYYMMDD Sample collection date, in year, month, day format. Producer Defined 20160829 20181023 Year, Month, Day (YYYYMMDD) D84_calculated Calculated D84 (large) particle size. 84% of the total particles are smaller than this size. Producer Defined NC Not calculated Producer defined 0.0036 0.0257 Millimeters 0.031_mm Percent of the analyzed sample that is less than 0.031 millimeters in diameter. Producer Defined NA Not applicable Producer defined 89.3 99.9 Percent 0.016_mm Percent of the analyzed sample that is less than 0.016 millimeters in diameter. Producer Defined NA Not applicable Producer defined 74.2 99.5 Percent 0.008_mm Percent of the analyzed sample that is less than 0.008 millimeters in diameter. Producer Defined NA Not applicable Producer defined 55.5 98.4 Percent 0.004_mm Percent of the analyzed sample that is less than 0.004 millimeters in diameter. Producer Defined NA Not applicable Producer defined 12.6 93.1 Percent 0.002_mm Percent of the analyzed sample that is less than 0.002 millimeters in diameter. Producer Defined NA Not applicable Producer defined 9.0 75.3 Percent 0.001_mm Percent of the analyzed sample that is less than 0.001 millimeters in diameter. Producer Defined NA Not applicable Producer defined 6.1 50.2 Percent LOI_Mass_g Lab measured Loss on Ignition: Mass of the sample that was burned off (organic matter content) before analysis, measured in grams. Producer Defined NA Not applicable Producer defined 0.263 0.758 Grams Sedigraph_Sediment_g Mass of the sediment sample used in the sedigraph particle size analysis. Producer Defined NA Not applicable Producer defined 1.6 2.8 Grams Plum_SedSAT_GeochemicalData.csv D50, LOI, and geochemistry data for SedSAT analysis. All elemental results are in mg/kg (ppm). Producer Defined FullName The sample name, completely written out. Producer Defined Recorded by basin, sample type, and sample number [Plum - Type - ##] format. Samples without sample numbers are either in [Plum - Type] or [Plum - Type - Location in Basin] format. These samples are differentiated by their collection date. Sample_ID Identification code of the sample analyzed. Producer Defined Identification code, recorded in basin, sample type, sample number, and collection date [PLCType##YYYYMMDD] format. Samples with out a sample number are in [PLCTypeYYYYMMDD] format. Date_YYYYMMDD Sample collection date, in year, month, day format. Producer Defined 20160829 20181023 Year, month, day (YYYYMMDD) SampleType The source or land use where the sample was collected. Producer Defined Bank Sediment collected from eroding streambank sections. Producer defined Bed Sediment collected from streambed soft sediment deposits. Producer defined Crop Sediment collected in agricultural or cropland land use areas. Producer defined SSEOF Suspended Sediment Edge of Field - Sediment collected with in-situ passive sediment samplers, located in the stream downstream of the USGS Edge of Field (EOF) site 44100088100001. Producer defined FESS Field - East Suspended Sediment - Sediment collected with in-situ passive sediment samplers, located on the ground in a swale draining the east side of the field at USGS Edge of Field (EOF) site 44100088100001. Producer defined FWSS Field - West Suspended Sediment - Sediment collected with in-situ passive sediment samplers, located on the ground in a swale draining the west side of the field at USGS Edge of Field (EOF) site 44100088100001. Producer defined Forest Sediment collected in woodland land use areas. Producer defined FOSS Forested Suspended Sediment - Sediment collected with in-situ passive sediment samplers, located in the stream in a forested setting on the east side of the basin. Producer defined SS Suspended Sediment - Sediment collected with in-situ passive sediment samplers, two sets of samplers located downstream of the bridge crossing near USGS gage 04084911 at Plum Creek. Producer defined GABE Sediment collected from streambed soft sediment deposits at USGS gage 04084911 at Plum Creek. Producer defined Gully Sediment collected in eroding gullies. Producer defined Roadway Sediment collected in grassy ditches between roads and fields. Producer defined URSS Urban Suspended Sediment - Sediment collected with in-situ passive sediment samplers, located in the stream in an urban, developed setting on the west side of the basin. Producer defined SSW Suspended Sediment West - Sediment collected with in-situ passive sediment samplers, located downstream of the bridge crossing near USGS gage 04084927 at West Plum Creek. Producer defined D50_calculated Calculated D50 (median) particle size. 50% of the total particles are smaller than this size. Producer Defined NC Not calculated Producer defined 0.00103 0.00749 Millimeters LOI_mg_kg Lab measured Loss on Ignition: Concentration of the sample that was burned off (organic matter content) before analysis, measured in milligrams per kilogram. Producer Defined NC Not calculated Producer defined 40200 210000 Milligrams per kilogram Li_ppm Sample lithium concentration. Producer Defined ND No Data Producer defined 20.1 56.9 Milligrams per kilogram, or parts per million (ppm) B_ppm Sample boron concentration. Producer Defined ND No Data Producer defined 34.7 121 Milligrams per kilogram, or parts per million (ppm) Na_ppm Sample sodium concentration. Producer Defined ND No Data Producer defined 3220 18800 Milligrams per kilogram, or parts per million (ppm) Mg_ppm Sample magnesium concentration. Producer Defined ND No Data Producer defined 1520 40700 Milligrams per kilogram, or parts per million (ppm) Al_ppm Sample aluminum concentration. Producer Defined ND No Data Producer defined 24800 73600 Milligrams per kilogram, or parts per million (ppm) P_ppm Sample phosphorus concentration. Producer Defined ND No Data Producer defined 467 1770 Milligrams per kilogram, or parts per million (ppm) S_ppm Sample sulfur concentration. Producer Defined ND No Data Producer defined 50 6370 Milligrams per kilogram, or parts per million (ppm) K_ppm Sample potassium concentration. Producer Defined ND No Data Producer defined 21900 39600 Milligrams per kilogram, or parts per million (ppm) Ca_ppm Sample calcium concentration. Producer Defined ND No Data Producer defined 5520 80500 Milligrams per kilogram, or parts per million (ppm) Sc_ppm Sample scandium concentration. Producer Defined ND No Data Producer defined 2.89 13.3 Milligrams per kilogram, or parts per million (ppm) Ti_ppm Sample titanium concentration. Producer Defined ND No Data Producer defined 2450 5620 Milligrams per kilogram, or parts per million (ppm) V_ppm Sample vanadium concentration. Producer Defined ND No Data Producer defined 55.3 113 Milligrams per kilogram, or parts per million (ppm) Cr_ppm Sample chromium concentration. Producer Defined ND No Data Producer defined 41.5 83.7 Milligrams per kilogram, or parts per million (ppm) Mn_ppm Sample manganese concentration. Producer Defined ND No Data Producer defined 284 2950 Milligrams per kilogram, or parts per million (ppm) Fe_ppm Sample iron concentration. Producer Defined ND No Data Producer defined 20300 48500 Milligrams per kilogram, or parts per million (ppm) Co_ppm Sample cobalt concentration. Producer Defined ND No Data Producer defined 5.94 19.1 Milligrams per kilogram, or parts per million (ppm) Ni_ppm Sample nickel concentration. Producer Defined ND No Data Producer defined 15.2 49.2 Milligrams per kilogram, or parts per million (ppm) Cu_ppm Sample copper concentration. Producer Defined ND No Data Producer defined 15.6 59.3 Milligrams per kilogram, or parts per million (ppm) Zn_ppm Sample zinc concentration. Producer Defined ND No Data Producer defined 48.6 271 Milligrams per kilogram, or parts per million (ppm) Ga_ppm Sample gallium concentration. Producer Defined ND No Data Producer defined 12 23.5 Milligrams per kilogram, or parts per million (ppm) As_ppm Sample arsenic concentration. Producer Defined ND No Data Producer defined 2.08 6.56 Milligrams per kilogram, or parts per million (ppm) Se_ppm Sample selenium concentration. Producer Defined ND No Data Producer defined 0.13 15.8 Milligrams per kilogram, or parts per million (ppm) Rb_ppm Sample rubidium concentration. Producer Defined ND No Data Producer defined 13.2 197 Milligrams per kilogram, or parts per million (ppm) Sr_ppm Sample strontium concentration. Producer Defined ND No Data Producer defined 76.2 782 Milligrams per kilogram, or parts per million (ppm) Y_ppm Sample yttrium concentration. Producer Defined ND No Data Producer defined 4.41 47.5 Milligrams per kilogram, or parts per million (ppm) Nb_ppm Sample niobium concentration. Producer Defined ND No Data Producer defined 9.31 18.8 Milligrams per kilogram, or parts per million (ppm) Mo_ppm Sample molybdenum concentration. Producer Defined ND No Data Producer defined 0.387 1.81 Milligrams per kilogram, or parts per million (ppm) Rh_ppm Sample rhodium concentration. Producer Defined ND No Data Producer defined 0.00131 0.0718 Milligrams per kilogram, or parts per million (ppm) Pd_ppm Sample palladium concentration. Producer Defined ND No Data Producer defined 0.231 6.53 Milligrams per kilogram, or parts per million (ppm) Ag_ppm Sample silver concentration. Producer Defined ND No Data Producer defined 0.207 1.74 Milligrams per kilogram, or parts per million (ppm) Cd_ppm Sample cadmium concentration. Producer Defined ND No Data Producer defined 0.175 0.694 Milligrams per kilogram, or parts per million (ppm) Sn_ppm Sample tin concentration. Producer Defined ND No Data Producer defined 1.41 17.2 Milligrams per kilogram, or parts per million (ppm) Sb_ppm Sample antimony concentration. Producer Defined ND No Data Producer defined 0.346 0.792 Milligrams per kilogram, or parts per million (ppm) Cs_ppm Sample cesium concentration. Producer Defined ND No Data Producer defined 1.86 4.11 Milligrams per kilogram, or parts per million (ppm) Ba_ppm Sample barium concentration. Producer Defined ND No Data Producer defined 296 738 Milligrams per kilogram, or parts per million (ppm) La_ppm Sample lanthanum concentration. Producer Defined ND No Data Producer defined 5.16 76.3 Milligrams per kilogram, or parts per million (ppm) Ce_ppm Sample cerium concentration. Producer Defined ND No Data Producer defined 11 130 Milligrams per kilogram, or parts per million (ppm) Pr_ppm Sample praseodymium concentration. Producer Defined ND No Data Producer defined 1.22 8.62 Milligrams per kilogram, or parts per million (ppm) Nd_ppm Sample neodymium concentration. Producer Defined ND No Data Producer defined 5.72 58.8 Milligrams per kilogram, or parts per million (ppm) Sm_ppm Sample samarium concentration. Producer Defined ND No Data Producer defined 1.09 12.4 Milligrams per kilogram, or parts per million (ppm) Eu_ppm Sample europium concentration. Producer Defined ND No Data Producer defined 0.308 1.90 Milligrams per kilogram, or parts per million (ppm) Dy_ppm Sample dysprosium concentration. Producer Defined ND No Data Producer defined 0.95 5.60 Milligrams per kilogram, or parts per million (ppm) Ho_ppm Sample holmium concentration. Producer Defined ND No Data Producer defined 0.193 1.15 Milligrams per kilogram, or parts per million (ppm) Yb_ppm Sample ytterbium concentration. Producer Defined ND No Data Producer defined 0.702 3.43 Milligrams per kilogram, or parts per million (ppm) W_ppm Sample tungsten concentration. Producer Defined ND No Data Producer defined 0.773 1.82 Milligrams per kilogram, or parts per million (ppm) Pt_ppm Sample platinum concentration. Producer Defined ND No Data Producer defined 0.0164 0.23 Milligrams per kilogram, or parts per million (ppm) Tl_ppm Sample thallium concentration. Producer Defined ND No Data Producer defined 0.456 0.928 Milligrams per kilogram, or parts per million (ppm) Pb_sum Sample lead concentration. Producer Defined ND No Data Producer defined 11 49.7 Milligrams per kilogram, or parts per million (ppm) Bi_ppm Sample bismuth concentration. Producer Defined ND No Data Producer defined 0.121 0.409 Milligrams per kilogram, or parts per million (ppm) Th_ppm Sample thorium concentration. Producer Defined ND No Data Producer defined 2.98 20.8 Milligrams per kilogram, or parts per million (ppm) U_ppm Sample uranium concentration. Producer Defined ND No Data Producer defined 2.18 5.20 Milligrams per kilogram, or parts per million (ppm) GS ScienceBase U.S. Geological Survey mailing address

Denver Federal Center, Building 810, Mail Stop 302

Denver CO 80225 United States 1-888-275-8747 sciencebase@usgs.gov Unless otherwise stated, all data, metadata and related materials are considered to satisfy the quality standards relative to the purpose for which the data were collected. Although these data and associated metadata have been reviewed for accuracy and completeness and approved for release by the U.S. Geological Survey (USGS), no warranty expressed or implied is made regarding the display or utility of the data on any other system or for general or scientific purposes, nor shall the act of distribution constitute any such warranty. Digital Data https://doi.org/10.5066/P13W43BB None 20250822 Heidi M Broerman U.S. Geological Survey, MIDCONTINENT REGION Physical Scientist mailing

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Madison Wisconsin 53726 United States 608-821-3818 hbroerman@usgs.gov FGDC Content Standard for Digital Geospatial Metadata FGDC-STD-001-1998